Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves

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URI: http://hdl.handle.net/10347/26821
ISBN: 3-906980-18-9
DOI: 10.3390/ecsoc-10-01442

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2006

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MDPI
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Microwave assisted organic synthesis (MAOS) of N,N-diisopropyl enol carbamate of acetophenone is achieved in good yield when acetophenone, N,N-diisopropylcarbamoyl chloride and Hüning's base, DABCO or TMEDA were irradiated with microwaves. It is remarkable that reaction times are reduced from six days with conventional heating, to twenty minutes

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The 10th International Electronic Conference on Synthetic Organic Chemistry session Symposium on Microwave Assisted Synthesis

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Seijas, J.A.; Vázquez-Tato, M.P.; Crecente-Campo, J. Studies on the base catalyzed synthesis of acetophenone enolcarbamate enhanced by microwaves, in Proceedings of the 10th International Electronic Conference on Synthetic Organic Chemistry, 1–30 November 2006, MDPI: Basel, Switzerland, doi:10.3390/ecsoc-10-01442

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XUNTA DE GALICIA for financial support: PGIDIT05PXIB26201PR, PR405 A 098/59-0 . USC for a predoctoral fellowship to JCC.

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©2007 by MDPI, Basel, Switzerland. Open Access

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Química Orgánica