Determination of pesticide residues in wine by solid-phase extraction on-line combined with liquid chromatography tandem mass spectrometry

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dc.contributor.affiliationUniversidade de Santiago de Compostela. Departamento de Química Analítica, Nutrición e Bromatoloxíagl
dc.contributor.authorPérez Mayán, Leticia
dc.contributor.authorRamil Criado, María
dc.contributor.authorCela Torrijos, Rafael
dc.contributor.authorRodríguez Pereiro, Isaac
dc.date.accessioned2021-09-23T12:19:11Z
dc.date.available2021-09-23T12:19:11Z
dc.date.issued2021
dc.description.abstractLiquid chromatography tandem mass spectrometry (LC–MS/MS) has been combined with different sample preparation strategies to determine potential pesticide residues existing in wine. Herein, we propose the on-line coupling between solid-phase extraction (SPE), based on a reversed-phase polystyrene-divinyl benzene (PS-DVB) sorbent, and LC–MS/MS for the automated monitoring of a selection of 48 pesticides (37 fungicides and 11 insecticides) in this beverage. Parameters affecting the sensitivity, selectivity, accuracy and robustness of the method are evaluated as function of sample volume, clean-up conditions, and number of extraction-desorption cycles performed with the same SPE cartridgegl
dc.description.peerreviewedSIgl
dc.description.sponsorshipL.P.M thanks a FPU grant to the Spanish Ministry of Science. This study was supported by Spanish Government and Xunta de Galicia through grants PGC2018-094613-B-I00 and ED431C 2021/06, both co- funded by the EU FEDER program. We acknowledge Agilent for providing access to the LC-ESI-MS/MS instrumentation employed in this studygl
dc.identifier.citationJournal of Food Composition and Analysis 104 (2021) 104184. https://doi.org/10.1016/j.jfca.2021.104184gl
dc.identifier.doi10.1016/j.jfca.2021.104184
dc.identifier.issn0889-1575
dc.identifier.urihttp://hdl.handle.net/10347/26945
dc.language.isoenggl
dc.publisherElseviergl
dc.relation.projectIDinfo:eu-repo/grantAgreement/AEI/Plan Estatal de Investigación Científica y Técnica y de Innovación 2017-2020/PGC2018-094613-B-I00/ES/ESPECTROMETRIA DE MASAS COMBINADA CON SISTEMAS DE INTRODUCCION DE MUESTRA RESUELTOS EN EL TIEMPO Y DIRECTOS. APLICACIONES ANALITICAS CUANTITATIVAS Y DE SCREENINGgl
dc.relation.publisherversionhttps://doi.org/10.1016/j.jfca.2021.104184gl
dc.rightsAttribution-NonCommercial-NoDerivatives 4.0 Internacional
dc.rights© 2021 The Authors. Published by Elsevier Inc. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/)gl
dc.rights.accessRightsopen accessgl
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/
dc.subjectPesticidesgl
dc.subjectWinegl
dc.subjectOn-line SPEgl
dc.subjectLiquid chromatographygl
dc.subjectTandem mass spectrometrygl
dc.titleDetermination of pesticide residues in wine by solid-phase extraction on-line combined with liquid chromatography tandem mass spectrometrygl
dc.typejournal articlegl
dc.type.hasVersionVoRgl
dspace.entity.typePublication
relation.isAuthorOfPublication05e62ba3-ed28-4ace-a2dc-9916ab3968a6
relation.isAuthorOfPublicationb3faf2dc-8b5b-458e-a409-9029aaa9fed1
relation.isAuthorOfPublication86047804-77ca-4036-ace6-2c953b7b6fd8
relation.isAuthorOfPublication.latestForDiscovery05e62ba3-ed28-4ace-a2dc-9916ab3968a6

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