The crystal structure of a compartmental heptadentate ligand

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2009_ecsoc13_fondo_crystal.pdf (139.94 KB)
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URI: http://hdl.handle.net/10347/26859
ISBN: 3-906980-23-5
DOI: 10.3390/ecsoc-13-00190

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2009

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MDPI
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2-(2-hydroxyphenyl)-1,3-bis[4-(2-hydroxyphenyl)-3-azabut-3-enyl]-1,3-imidazolidine (H3L) was obtained with high purity by Schiff's condensation between 5-bromosalicyaldehyde and triethylenetetramine. Its recrystallisation in methanol yields single crystals suitable for X-ray diffraction studies. H3L crystallises in the monoclinic system, space group P21/c, with a = 21.641(3) Å, b = 11.1217(14) Å, c = 11.4156(15) Å and β = 90.016 º

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The 13th International Electronic Conference on Synthetic Organic Chemistry session General Organic Synthesis

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Sanmartín, J.; García-Deibe, A.M.; Ocampo, N.; Fondo, M. The crystal structure of a compartmental heptadentate ligand, in Proceedings of the 13th International Electronic Conference on Synthetic Organic Chemistry, 1–30 November 2009, MDPI: Basel, Switzerland, doi:10.3390/ecsoc-13-00190

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© 2009 The author(s). Published by MDPI, Basel, Switzerland. Open Access

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Química Inorgánica