9H-Dibenzo[a,c]carbazole from microwave assisted Madelung\'s reaction of N-[2-(phenylmethyl)phenyl]benzamide
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Abstract
Microwave irradiation of N-[2-(phenylmethyl)phenyl]benzamide with potassium tert-butoxide leads to a 1:1 ratio of the expected product from Madelung's reaction and 9H-Dibenzo[a,c]carbazole. This one seems to come from a competitive reaction pathway rather than from thermal conrotatory electrocyclic of 2,3-diphenyl- 3H-Indole
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The 13th International Electronic Conference on Synthetic Organic Chemistry session Symposium on Microwave Assisted Synthesis
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Núñez-Álvarez, L.; Gómez- Doval, M.; Crecente-Campo, J.; Vázquez-Tato, M.; Seijas, J.A. 9H-Dibenzo[a,c]carbazole from microwave assisted Madelung\'s reaction of N-[2-(phenylmethyl)phenyl]benzamide, in Proceedings of the 13th International Electronic Conference on Synthetic Organic Chemistry, 1–30 November 2009, MDPI: Basel, Switzerland, doi:10.3390/ecsoc-13-00160
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https://doi.org/10.3390/ecsoc-13-00160Sponsors
XUNTA DE GALICIA for financial support: PGIDIT05PXIB26201PR and USC for a predoctoral fellowship to JCC
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© 2009 The author(s). Published by MDPI, Basel, Switzerland. Open Access